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13C谱最新氘代试剂(核磁试剂)化学位移表

13C谱最新氘代试剂（核磁试剂）化学位移表
2010-7-17
13C氘代试剂（核磁试剂）化学位移表
碳原子
氘代四氢呋喃
氘代二氯甲烷
氘代氯仿
氘代甲苯
氘代苯
氘代氯苯
氘代丙酮
氘代DMSO
氘代乙腈
氘代三氟乙醇
氘代甲醇
氘代水
氘代试剂位移
67.21
53.84
77.16
137.48
128.06
134.19
29.84
39.52
1.32
61.50
49.00
 
 
 
25.31
 
 
128.87
 
129.26
206.26
 
118.26
126.28
 
 
 
 
 
 
 
127.96
 
128.25
 
 
 
 
 
 
 
 
 
 
 
125.13
 
125.96
 
 
 
 
 
 
 
 
 
 
 
20.43
 
 
 
 
 
 
 
 
乙酸
CO
171.69
175.85
175.99
175.30
175.82
175.67
172.31
171.93
173.21
177.96
175.11
177.21
 
CH3
20.13
20.91
20.81
20.27
20.37
20.40
20.51
20.95
20.73
20.91
20.56
21.03
丙酮
CO
204.19
206.78
207.07
204.00
204.43
204.83
205.87
206.31
207.43
32.35
209.67
215.94
 
CH3
30.17
31.00
30.92
30.03
30.14
30.12
30.60
30.56
30.91
214.98
30.67
30.89
乙腈
CN
116.79
116.92
116.43
115.76
116.02
115.93
117.60
117.91
118.26
118.95
118.06
119.68
 
CH3
0.45
2.03
1.89
0.03
0.20
0.63
1.12
1.03
1.79
1.00
0.85
1.47
苯
CH
128.84
128.68
128.37
128.57
128.62
128.38
129.15
128.30
129.32
129.84
129.34
 
正丁醇
(CH3)3C
67.50
69.11
69.15
68.12
68.19
68.19
68.13
66.88
68.74
72.35
69.40
70.36
 
(CH3)3C
30.57
31.46
31.25
30.49
30.47
31.13
30.72
30.38
30.68
31.07
30.91
30.29
二甘醇二甲醚
CH3
58.72
58.95
59.01
58.62
58.66
58.42
58.77
57.98
58.90
59.40
59.06
58.67
 
CH2
71.17
70.70
70.51
70.92
70.87
70.56
71.03
69.54
70.99
73.05
71.33
70.05
 
CH2
72.72
72.25
71.90
72.39
72.35
72.07
72.63
71.25
72.63
71.33
72.92
71.63
二甲基甲酰胺
CH
161.96
162.57
162.62
161.93
162.13
162.01
162.79
162.29
163.31
166.01
164.73
165.53
 
CH3
35.65
36.56
36.50
35.22
35.25
35.45
36.15
35.73
36.57
37.76
36.89
37.54
 
CH3
30.70
31.39
31.45
30.64
30.72
30.71
31.03
30.73
31.32
30.96
31.61
32.03
1,4-二恶烷
CH2
67.65
67.47
67.14
67.17
67.16
66.95
67.60
66.36
67.72
68.52
68.11
67.19
DME
CH3
58.72
59.02
59.08
58.63
58.68
58.31
58.45
58.03
58.89
59.52
59.06
58.67
 
CH2
72.58
72.24
71.84
72.25
72.21
71.81
72.47
71.17
72.47
72.87
72.72
71.49
乙烷
CH3
6.79
6.91
6.89
6.94
6.96
6.91
6.88
6.61
6.99
7.01
6.98
 
乙醇
CH3
18.90
18.69
18.41
18.78
18.72
18.55
18.89
18.51
18.80
18.11
18.40
17.47
 
CH2
57.60
58.57
58.28
57.81
57.86
57.63
57.72
56.07
57.96
59.68
58.26
58.05
二氧化碳
CO2
125.69
125.26
124.99
124.86
124.76
126.08
125.81
124.21
125.89
126.92
126.31
 
二硫化碳
CS2
193.37
192.95
192.83
192.71
192.69
192.49
193.58
192.63
193.60
196.26
193.82
197.25
四氯化碳
CCl4
96.89
96.52
96.34
96.57
96.44
96.38
96.65
95.44
96.68
97.74
97.21
96.73
氯仿
CH
79.24
77.99
77.36
77.89
77.79
77.67
79.19
79.16
79.17
78.83
79.44
 
18-冠醚-6
CH2
71.34
70.47
70.55
70.86
70.59
70.55
71.25
69.85
71.22
70.80
71.47
70.14
环己胺
CH2
27.58
27.38
26.94
27.31
27.23
26.99
27.51
26.33
27.63
28.34
27.96
 
二氯乙烷
CH2
44.64
44.35
43.50
43.40
43.59
43.60
45.25
45.02
45.54
45.28
45.11
 
二氯甲烷
CH2
54.67
54.24
53.52
53.47
53.46
53.54
54.95
54.84
55.32
54.46
54.78
 
乙醚
CH3
15.49
15.44
15.20
15.47
15.46
15.35
15.78
15.12
15.63
15.33
15.46
14.77
 
CH2
66.14
66.11
65.91
65.94
65.94
65.79
66.12
62.05
66.32
67.55
66.88
66.42
乙酸乙酯
CH3CO
20.45
21.15
21.04
20.46
20.56
20.50
20.83
20.68
21.16
21.18
20.88
21.15
 
CO
170.32
171.24
171.36
170.02
170.44
170.20
170.96
170.31
171.68
175.55
172.89
175.26
 
CH2
60.30
60.63
60.49
60.08
60.21
60.06
60.56
59.74
60.98
62.70
61.50
62.32
 
CH3
14.37
14.37
14.19
14.23
14.19
14.07
14.50
14.40
14.54
14.36
14.49
13.92
乙烯
CH2
123.09
123.20
123.13
122.92
122.96
122.95
123.47
123.52
123.69
, 124.08
123.46
 
乙二醇
CH2
64.35
63.79
64.29
64.34
64.03
64.26
62.76
64.22
64.87
64.30
63.17
H greaseb
CH2
30.45
30.14
29.71
30.31
30.22
30.11
 
 
菲特台风路径 
 
 
 
六甲基苯
C
131.88
132.09
132.21
131.72
131.79
131.54
132.22
131.10
132.61
134.04
132.53
 
 
CH3
16.71
16.93
16.98
16.84
16.95
16.68
16.86
16.60
16.94
17.04
16.90
 
正己烷
CH3
14.22
14.28
14.14
14.34
14.32
14.18
14.34
干事创业13.88
14.43
14.63
14.45
 
 
CH2(2,5)
23.33
23.07
22.70
23.12
23.04
22.86
23.28
22.05
23.40
24.06
23.68
 
 
CH2(3,4)
32.34
32.01
31.64
32.06
31.96
31.77
32.30
30.95
32.36
33.17
32.73
安阳榕树湾
吡咯
CH(2,5)
118.03
117.93
117.77
117.61
117.78
117.65
117.98
117.32
118.47
119.61
118.28
119.06
 
CH(3,4)
107.74
108.02
107.98
108.15
108.21
108.03
108.04
107.07
108.31
108.85
108.11
107.83
吡咯啉
CH2(2,5)
45.82
47.02
46.93
47.12
46.86
46.75
 
46.51
47.57
47.43
47.23
46.83
 
CH2(3,4)
26.17
25.83
25.56
25.75
25.65
25.59
 
25.26
26.34
25.73
26.29
25.86
硅脂
CH3
1.20
1.22
1.19
1.37
1.38
钻采工艺
1.09
1.40供配电
 
 
2.87
2.10
 
四氢呋喃
CH2(2,5)
68.03
68.16
67.97
67.75
67.80
67.64
68.07
67.03
68.33
69.53
68.83
68.68
 
CH2(3,4)
26.19
25.98
25.62
25.79
25.72
25.68
26.15
25.14
26.27
26.69
26.48
25.67
甲苯
CH3
21.29
21.53
21.46
21.37
21.10
21.23
21.46
20.99
21.50
21.62
21.50
 
 
C(1)
138.24
138.36
137.89
137.84
137.91
137.65
138.48
137.35
138.90
139.92
138.85
 
 
CH(2,6)
129.47
129.35
129.07
129.33
129.33
129.12
129.76
128.88
129.94
130.58
129.91
 
 
CH(3,5)
128.71
128.54
128.26
128.51
128.56
128.31
129.03
128.18
129.23
129.79
129.20
 
 
CH(4)
125.84
125.62
125.33
125.66
125.68
125.43
126.12
125.29
126.28
126.82
126.29
 
三乙胺
CH3
12.51
12.12
11.61
12.39
12.35
11.87
12.49
11.74
12.38
9.51
11.09
9.07
 
CH2
47.18
46.75
46.25
46.82
46.77
46.36
47.07
45.74
47.10
48.45
46.96
47.19
六甲基二硅醚
CH3
1.83
1.96
1.97
1.99
2.05
1.92
2.01
1.96
2.07
2.09
1.99
2.31
HMPAc
CH3
36.89
36.99
36.87
36.80
36.88
36.64
37.04
36.42
37.10
37.21
37.00
36.46
咪唑
CH(2)
135.72
135.76
135.38
135.57
135.76
135.50
135.89
135.15
136.33
136.58
136.31
136.65
 
CH(4,5)
122.20
122.16
122.00
122.13
122.16
121.96
122.31
121.55
122.78
122.93
122.60
122.43
甲烷
CH4
-4.90
-4.33
-4.63
-4.34
-4.29
-4.33
-5.33
-4.01
-4.61
-5.88
-4.90
 
甲醇
CH3
49.64
50.45
50.41
49.90
49.97
49.66
49.77
48.59
49.90
50.67
49.86
49.50d
硝基甲烷
CH3
62.49
63.03
62.50
61.14
61.16
61.68
63.21
63.28
63.66
63.17
63.08
63.22
正戊烷
CH3
14.18
14.24
14.08
14.27
14.25
14.10
14.29
13.28
14.37
14.54
14.39
 
 
CH2(2,4)
23.00
22.77
22.38
22.79
22.72
22.54
22.98
21.70
23.08
23.75
23.38
 
 
CH2(3)
34.87
34.57
34.16
34.54
34.45
34.26
34.83
33.48
34.89
35.76
35.30
 
丙烷
CH3
16.60
16.63
16.63
16.65
16.66
16.56
16.68
16.34
16.73
16.93
16.80
 
 
CH2
16.82
16.63
16.37
16.63
16.60
16.48
16.78
15.67
16.91
17.46
17.19
 
2-丙醇
CH3
25.70
25.43
25.14
25.24
25.18
25.14
25.67
25.43
25.55
女体解剖图
25.21
25.27
24.38
 
CH
66.14
64.67
64.50
64.12
64.23
64.18
63.85
64.92
64.30
66.69
64.71
64.88
丙烯
CH3
19.27
19.47
19.50
19.32
19.38
19.32
19.42
19.20
19.48
19.63
19.50
 
 
CH2
115.74
115.70
115.74
115.89
115.92
115.86
116.03
116.07
116.12
116.38
116.04
 
 
CH
134.02
134.21
133.91
133.61
133.69
133.57
134.34
133.55
134.78
136.00
134.61
 
吡啶
CH(2,6)
150.57
150.27
149.90
150.25
150.27
149.93
150.67
149.58
150.76
149.76
150.07
149.18
 
CH(3,5)
124.08
124.06
123.75
123.46
123.58
123.49
124.57
123.84
127.76
126.27
125.53
125.12
 
CH(4)
135.99
136.16
135.96
135.17
135.28
135.32
136.56
136.05
136.89
139.62
138.35
138.2
          以上为核磁共振碳谱中氘代试剂及常用溶剂在相应氘代试剂中的化学位移。

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