File D:\CHEM32\1\DATA\BIZ\BIZ2016-N03-WJ10.D Tgt Mass (EZX): 461.00 Injection Date : 3 Nov 16 4:37 pm +0800 Seq. Line : 0 Sample Name : BIZ2016-N03-WJ10 Location : P2-B-05 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M
Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M
&DWDORJ 1R +< %DWFK Easy-Access Method: '1-POS-3MIN' 461.00 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min
孙荣章Column :SunFire C18, 4.6*50mm,3.5um A-RP-186
Oven Temperature : 45C
min*
0.5
1
1.5
2 2.5mAU 0
5001000
1500*DAD1 B, Sig=214,4 Ref=off
1.632
高频变压器
设计软件2.017
2.190
min*
0.51
1.5
2 2.5mAU 0
200400600800*DAD1 C, Sig=254,4 Ref=off 1.632
2.006
2.190
min
0.51 1.5
2
2.5
100000
200000300000400000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70
1.626
min
0.5
1
1.5
2
50000
100000 Ion 462, MSD1 462,Target Mass 461 +H Positive, EIC=461.7:462.7
1.627
Integration Results for DAD1 B, Sig=214,4 Ref=off
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.63 0.02 1990.52 1902.57 99.15 462 2.02 0.02 9.93 7.01 0.49 233 2.19 0.02 7.23 5.03 0.36 233
Integration Results for DAD1 C, Sig=254,4 Ref=off
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.63 0.02 1045.42 1007.92 99.47 462 2.01 0.02 2.61 2.10 0.25 233 2.19 0.02 3.01 2.35 0.29 233
Ret. Time: 1.63 <<<< POSITIVE SPECTRA >>>>
m/z
200
300
400
500
600
71岁过芭蕾六级700
800
900
5000
10000150002000025000
3000035000 ES-API Positive
294.1卵黄磷蛋白
233.1
945.2
232.6
231.6
空气净化
高压电源465.2 484.2 464.1 462.2
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