=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 90
Acq. Instrument : HY-LCMS-02 Location : P2-F-01Injection Date : 7/29/2015 8:07:55 PM Inj : 1
Inj Volume : 3.000 µl
Acq. Method : D:\AGLIENT 1260\DATA\20150729\20150729 2015-07-29 10-28-13\100-1000MS+3MIN- 1.5_(0.02%FA).M
Last changed : 7/29/2015 10:28:13 AM by Li Shan(LCMS-02)
Analysis Method : D:\AGLIENT 1260\DATA\20150722\20150722 2015-07-22 10-02-30\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)
Last changed : 7/30/2015 4:14:07 PM by Li Shan(LCMS-02) (modified after loading)
Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃
Catalog No : HY-10320 Batch#17233 A-RP-134
Additional Info : Peak(s) manually integrated
min
0.5
1
2 2.53mAU 0
柯尔特m2000
5001000
15002000 DAD1 B, Sig=214,4 Ref=off (D:\0\DATA\20150729\20150729 2015-07-29 10-28-13\BIZ2015-729-DJL17.D)
1.668
2.047
2.142标准布朗运动
2.414
2.568
2.792 2.861
===================================================================== Area Percent Report =====================================================================
Sorted By : Signal Multiplier : 1.0000Dilution : 1.0000
小小说月刊
Do not use Multiplier & Dilution Factor with ISTDs
Signal 1: DAD1 B, Sig=214,4 Ref=off
Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %
----|-------|----|-------|----------|----------|--------| 1 1.668 MM 0.0707 9.73165 2.29552 0.1191 2 2.047 MM 0.0494 3.61731 1.21929 0.0443 3 2.142 MM 0.0524 8120.56055 2583.23999 9
9.3983 4 2.414 MM 0.0740 11.14499 2.51139 0.1364 5 2.568 MM 0.0640 7.66619 1.99720 0.0938 6 2.792 MM 0.0550 12.74362 3.86362 0.1560 7 2.861 MM 0.0462 4.25446 1.53477 0.0521
Totals : 8169.71876 2596.66177
===================================================================== *** End of Report ***
=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 90
Acq. Instrument : HY-LCMS-02 Location : P2-F-01Injection Date : 7/29/2015 8:07:55 PM Inj : 1
Inj Volume : 3.000 µl
Acq. Method : D:\AGLIENT 1260\DATA\20150729\20150729 2015-07-29 10-28-13\100-1000MS+3MIN- 1.5_(0.02%FA).M
Last changed : 7/29/2015 10:28:13 AM by Li Shan(LCMS-02)
Analysis Method : D:\AGLIENT 1260\DATA\20150722\20150722 2015-07-22 10-02-30\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)
Last changed : 7/30/2015 4:15:08 PM by Li Shan(LCMS-02) (modified after loading)
Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃
Catalog No : HY-10320 Batch#17233 A-RP-134
Additional Info : Peak(s) manually integrated
min
0.5
1
1.5
2
2.5
3
100000
200000300000400000500000 MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20150729\20150729 2015-07-29 10-28-13\BIZ2015-729-DJL17.D) ES-API, Pos, Sca
2.143
MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts.
Reportable Ion Abundance: > 10%.
Retention Mol. Weight Time (MS) MS Area or Ion
2.143 2287306 529.30 I 528.30 I 264.70 I
m/z
100
200
300
400
500
600
700
800
900
20406080100*MSD1 SPC, time=2.127:2.163 of D:\AGLIENT 1260\DATA\20150729\20150729 2015-07-29 10-28-13\BIZ2015-729-DJL17.D ES-API Max: 252352
529.3 528.3
麦博md332264.7
*** End of Report ***
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