File ..3\Data\20170914\20170914 5\LCP4661-002-3A.D Tgt Mass (CHM): Injection Date : 14 Sep 17 2:41 pm +0800 Seq. Line : 15 Sample Name : LCP4661-002-3A Location : P2-C-02 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\LCMS03\Data\20170914\20170914 5\1-POS-3MIN.M Analysis Method : D:\LCMS03\Data\20170914\20170914 5\1-POS-3MIN.M Catalog No : HY-13631A Batch#26303 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C
min 00.5
1 1.5
2 2.5mAUcsg
500
DAD1 A, Sig=214,4 Ref=off
1.1941.2431.362min 00.5
1 1.5
2 2.5mAU
200
400
DAD1 B, Sig=254,4 Ref=off
1.1941.2531.342min 00.51
1.52
2.5mV
50
ELS1 A, ELSD Signal
1.258min
00.51
1.52
2.50
2000000
吹牛的由来4000000
MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70
1.2241.670min 00.51 1.52
2.5-0.1
-0.05
0.05
Ion 0, MSD1 0,Target Mass 0 Positive, EIC=-0.30:0.70
Integration Results for DAD1 A, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.19 0.02 1069.56 929.90 98.03 436 1.24 0.03 12.34 -1.12 1.13 436 1.36 0.04 9.18 3.86 0.84 292
Integration Results for DAD1 B, Sig=254,4 Ref=off
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.19 0.02 796.35 694.17 98.12 436 1.25 0.01 12.31 17.86 1.52 436 1.34 0.06 2.93 1.80 0.36 292
Integration Results for MSD1 TIC, MS File
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.22 0.07 24381116.00 5512260.00 99.02 436 1.67 0.05 242489.44 -1305.52 0.98 245
Ret. Time: 1.22 <<<< POSITIVE SPECTRA >>>>m/z 1002003004005006007008009000
100000200000
300000
400000500000600000*ES-API Positive
438.1437.2894.3436.2
Ret. Time: 1.67
m/z 1002003004005006007008009000
5000
10000
县域黑社会生存之道15000
20000
25000
30000
35000
淡漠如烟
夫妻店ES-API Positive
284.1344.2
单乙醇胺112.1436.2326.1
中国
教育改革和
发展纲要
408.3
138.1
235.0
261.1
372.2
217.1
141.1349.2105.1
371.2245.1
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