File ..0622 2017-06-22 08-39-15\BIZ2017-621-WYQ4.D Tgt Mass (CHM): Injection Date : 22 Jun 17 9:32 am +0800 Seq. Line : 12 Sample Name : BIZ2017-621-WYQ4 Location : P2-B-05 Acq. Operator : CLJ_701 Inj : 1 Spec. Reported : MS Integration Inj Volume : 0.5 ul
Acq. Method : D:\chem32\1\DATA\20170622\20170622 2017-06-22 08-39-15\1-POS-3MIN.M Analysis Method : D:\CHEM32\1\DATA\20170622\20170622 2017-06-22 08-39-15\1-POS-3MIN.M Catalog No : HY-N0527 Batch#25047 A-RP-186
Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min
Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C
min
0.5
1
1.52
msinfo
2.5mAU 0
5001000 DAD1 B, Sig=214,4 Ref=off
1.200
1.2521.3361
.3562.035
min
0.51
1.52
2.5mAU 0
50100150 DAD1 C, Sig=254,4 Ref=off 0.443
1.201
1.252
1.319
2.073
min
0.51 1.5
2 2.55000
1000015000
2000025000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70
1.242
min
0.5
1
1.5
2 2.50
50100150200 Ion 941.1, MSD1 941.1,Target Mass 940.1 +H Positive, EIC=940.8:941.8 Integration Results for DAD1 B, Sig=214,4 Ref=off
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.20 0.02 6.21 5.21 0.35 344 1.25 0.02 1758.55 1461.23 99.04 ND 1.34 0.02 7.10 6.08 0.40 ND 1.36 0.02 3.04 2.35 0.17 ND 2.04 0.02 0.70 0.56 0.04 233
Integration Results for DAD1 C, Sig=254,4 Ref=off
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.44 0.47 0.48 0.36 0.17 ND 1.20 0.06 0.83 0.75 0.30 344 1.25 0.02 273.84 228.84 98.69 ND 1.32 0.05 1.64 1.49 0.59 ND 2.07 0.02 0.69 0.55 0.25 233
Integration Results for MSD1 TIC, MS File
RetTim Width Area Height Area% MS(+)
MS Report from Instrument: LCMS-02
MS Report from Instrument: LCMS-02
|-------|--------|--------------|--------------|--------|------| 1.24 0.08 32500.54 6788.87 100.00 ND
=====================================================================Acq. Operator : CLJ_701 Seq. Line : 12
Acq. Instrument : LCMS-02 Location : P2-B-05Injection Date : 6/22/2017 9:32:32 Inj : 1
Inj Volume : 1.000 µl Different Inj Volume from Sample Entry! Actual Inj Volume : 0.500 µl
Acq. Method : D:\CHEM32\1\DATA\20170622\20170622 2017-06-22 08-39-15\1-POS-3MIN.M Last changed : 6/22/2017 8:39:15 by CLJ_701
Analysis Method : D:\CHEM32\1\DATA\20170622\20170622 2017-06-22 08-39-15\1-POS-3MIN.M (Sequence Method)
Last changed : 6/22/2017 10:18:44 by CLJ_701 (modified after loading)
Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min
Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C
Catalog No : HY-N0527 Batch#25047 A-RP-186
Additional Info : Peak(s) manually integrated
min
0.5
1
1.5
2
2.5
5000
75001000012500150001750020000
2250025000 MSD1 TIC, MS File (D:\CHEM32\1\DATA\20170622\20170622 2017-06-22 08-39-15\BIZ2017-621-WYQ4.D) ES-API, Pos, Scan, Fr
1.242
MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 70 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts.
Reportable Ion Abundance: > 10%.
Retention Mol. Weight Time (MS) MS Area or Ion
1.242 32501 388.20 I
m/z
100
200
300
400
500
600
700
800
900
2040
6080100*MSD1 SPC, time=1.179:1.257 of D:\CHEM32\1\DATA\20170622\20170622 2017-06-22 08-39-15\BIZ2017-621-WYQ4.D ES-API, Pos
Max: 1037
139.9 114.1
852.1
281.4 390.0 301.0
481.0
162.9
636.7
409.3
742.4
521.3
239.0 195.1
345.2
437.0
371.0 327.0 233.1
393.1 141.0
476.1
317.1
279.1
344.2
432.2
388.2
*** End of Report ***
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